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Allyl phosphorodichloridothionate, which is the starting material for esters of this acid, was obtained by Pletz [146] by the addition of sulphur to allyl phosphorodichloridite, and by the treatment of thiophosphoryl chloride with allyl alcohol: CH2 = CHCH20PC12 + Sv * CH2 = CHCH20PSC12 CH2 ■= CHCH2OH+PSCL/* However, unsaturated esters of phosphorothionic acid are, as a rule, synthesized by the addition of sulphur to the corresponding trialkenyl phos­ phite [91, 111, 121]. Triallyl phosphorothionate PS(OCH 2 CH = CH 2 ) 3 [111] P(OCH2CH = CH2)3 + S ► PS(OCH2CH = CH2)3 Finely ground crystalline sulphur (3 • 2 g) was added to triallyl phosphite (20«2g): an exothermic reaction proceeded on mixing, and all the sulphur dissolved.

Triallyl phosphorothionate PS(OCH 2 CH = CH 2 ) 3 [111] P(OCH2CH = CH2)3 + S ► PS(OCH2CH = CH2)3 Finely ground crystalline sulphur (3 • 2 g) was added to triallyl phosphite (20«2g): an exothermic reaction proceeded on mixing, and all the sulphur dissolved. Distillation afforded triallyl phosphorothionate (18- 87 g, 80-6%), b. p . 125-127°/9 mm, n]? 14832, d™ 1-0827. The 3-chloropropenyl esters of dialkyl hydrogen phosphorothiolothionates were obtained by Tichy [147] by the reaction of salts of these acids with l,3-dichlorobut-2-ene and soda.

P. 93-94°/l mm, 7i2^ 1 ^4500, df 1-0815. Allyl phosphorodichloridothionate, which is the starting material for esters of this acid, was obtained by Pletz [146] by the addition of sulphur to allyl phosphorodichloridite, and by the treatment of thiophosphoryl chloride with allyl alcohol: CH2 = CHCH20PC12 + Sv * CH2 = CHCH20PSC12 CH2 ■= CHCH2OH+PSCL/* However, unsaturated esters of phosphorothionic acid are, as a rule, synthesized by the addition of sulphur to the corresponding trialkenyl phos­ phite [91, 111, 121].

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